Direct synthesis of highly stable mesoporous molecular sieves containing zeolite building units

Ayyamperumal Sakthivel; Shing Jong Huang; Wen Hua Chen; Zon Huang Lan; Kuei Hsien Chen; Hong Ping Lin; Chung Yuan Mou; Shang Bin Liu

doi:10.1002/adfm.200400038

Direct synthesis of highly stable mesoporous molecular sieves containing zeolite building units

Ayyamperumal Sakthivel, Shing Jong Huang, Wen Hua Chen, Zon Huang Lan, Kuei Hsien Chen, Hong Ping Lin, Chung Yuan Mou, Shang Bin Liu

Research output: Contribution to journal › Article › peer-review

56 Citations (Scopus)

Abstract

A novel, one-step synthesis of a highly stable mesoporous molecular sieve (MMS-H), which has a structure analogous to MCM-48 but which contains zeolite building units, is reported. A variety of experimental techniques-X-ray diffraction (XRD), N₂ adsorption/desorption, transmission electron microscopy (TEM), Fourier-transform infrared (FTIR) spectroscopy, hyperpolarized ¹²⁹XeNMR, and solid-state ²⁷Al and ³¹P magic-angle spinning (MAS) NMR spectroscopies - have been used to characterize the framework structure, porosity, and acidity of this novel mesoporous/microporous composite material, which is also found to possess superior thermal, hydrothermal, steam, and mechanical stabilities.

Original language	English
Pages (from-to)	253-258
Number of pages	6
Journal	Advanced Functional Materials
Volume	15
Issue number	2
DOIs	https://doi.org/10.1002/adfm.200400038
Publication status	Published - Feb 2005
Externally published	Yes

ASJC Scopus subject areas

General Chemistry
General Materials Science
Condensed Matter Physics

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10.1002/adfm.200400038

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abstract = "A novel, one-step synthesis of a highly stable mesoporous molecular sieve (MMS-H), which has a structure analogous to MCM-48 but which contains zeolite building units, is reported. A variety of experimental techniques-X-ray diffraction (XRD), N2 adsorption/desorption, transmission electron microscopy (TEM), Fourier-transform infrared (FTIR) spectroscopy, hyperpolarized 129XeNMR, and solid-state 27Al and 31P magic-angle spinning (MAS) NMR spectroscopies - have been used to characterize the framework structure, porosity, and acidity of this novel mesoporous/microporous composite material, which is also found to possess superior thermal, hydrothermal, steam, and mechanical stabilities.",

author = "Ayyamperumal Sakthivel and Huang, {Shing Jong} and Chen, {Wen Hua} and Lan, {Zon Huang} and Chen, {Kuei Hsien} and Lin, {Hong Ping} and Mou, {Chung Yuan} and Liu, {Shang Bin}",

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AU - Sakthivel, Ayyamperumal

AU - Huang, Shing Jong

AU - Chen, Wen Hua

AU - Lan, Zon Huang

AU - Chen, Kuei Hsien

AU - Lin, Hong Ping

AU - Mou, Chung Yuan

AU - Liu, Shang Bin

PY - 2005/2

Y1 - 2005/2

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AB - A novel, one-step synthesis of a highly stable mesoporous molecular sieve (MMS-H), which has a structure analogous to MCM-48 but which contains zeolite building units, is reported. A variety of experimental techniques-X-ray diffraction (XRD), N2 adsorption/desorption, transmission electron microscopy (TEM), Fourier-transform infrared (FTIR) spectroscopy, hyperpolarized 129XeNMR, and solid-state 27Al and 31P magic-angle spinning (MAS) NMR spectroscopies - have been used to characterize the framework structure, porosity, and acidity of this novel mesoporous/microporous composite material, which is also found to possess superior thermal, hydrothermal, steam, and mechanical stabilities.

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Direct synthesis of highly stable mesoporous molecular sieves containing zeolite building units

Abstract

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