Calcium hydroxyapatite/whitlockite obtained from dairy products: Simple, environmentally benign and green preparation technology

J. Trinkunaite-Felsen; Z. Stankeviciute; J. C. Yang; Thomas C.K. Yang; A. Beganskiene; A. Kareiva

doi:10.1016/j.ceramint.2014.04.120

Calcium hydroxyapatite/whitlockite obtained from dairy products: Simple, environmentally benign and green preparation technology

J. Trinkunaite-Felsen
, Z. Stankeviciute
, J. C. Yang
, Thomas C.K. Yang
, A. Beganskiene
, A. Kareiva

Research output: Contribution to journal › Article › peer-review

27 Citations (Scopus)

Abstract

This study presents synthesis and characterization of calcium hydroxyapatite (Ca₁₀(PO₄)₆(OH)₂, CHAp) and whitlockite (Ca₁₈Mg₂H₂(PO ₄)₁₄) composite obtained from dairy product. First, calcium containing powders were precipitated from whey permeate by combining the effect of alkaline pH and temperature. Subsequently a calcium containing phase was collected using membrane filtration and spray-dried. Finally, the temperature treatment was applied to eliminate the organic phase and purify calcium containing compounds. The mechanism of thermal decomposition of dairy calcium powder (DCP) was investigated using thermogravimetric analysis coupled with differential scanning calorimetry (TG-DSC). The phase composition, structural and morphological features of the final products were studied by X-ray diffraction analysis (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM).

Original language	English
Pages (from-to)	12717-12722
Number of pages	6
Journal	Ceramics International
Volume	40
Issue number	8 PART B
DOIs	https://doi.org/10.1016/j.ceramint.2014.04.120
Publication status	Published - Sept 2014

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

SDG 9 Industry, Innovation, and Infrastructure

Keywords

Bioceramic materials
Calcium hydroxyapatite
Dairy products
Green manufacturing
Whitlockite

ASJC Scopus subject areas

Electronic, Optical and Magnetic Materials
Ceramics and Composites
Process Chemistry and Technology
Surfaces, Coatings and Films
Materials Chemistry

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10.1016/j.ceramint.2014.04.120

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@article{6b047045a9fc46888d1c700bd8acebba,

title = "Calcium hydroxyapatite/whitlockite obtained from dairy products: Simple, environmentally benign and green preparation technology",

abstract = "This study presents synthesis and characterization of calcium hydroxyapatite (Ca10(PO4)6(OH)2, CHAp) and whitlockite (Ca18Mg2H2(PO 4)14) composite obtained from dairy product. First, calcium containing powders were precipitated from whey permeate by combining the effect of alkaline pH and temperature. Subsequently a calcium containing phase was collected using membrane filtration and spray-dried. Finally, the temperature treatment was applied to eliminate the organic phase and purify calcium containing compounds. The mechanism of thermal decomposition of dairy calcium powder (DCP) was investigated using thermogravimetric analysis coupled with differential scanning calorimetry (TG-DSC). The phase composition, structural and morphological features of the final products were studied by X-ray diffraction analysis (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM).",

keywords = "Bioceramic materials, Calcium hydroxyapatite, Dairy products, Green manufacturing, Whitlockite",

author = "J. Trinkunaite-Felsen and Z. Stankeviciute and Yang, \{J. C.\} and Yang, \{Thomas C.K.\} and A. Beganskiene and A. Kareiva",

note = "Funding Information: Postdoctoral fellowship of Z.S. is being funded by European Union Structural Funds Project {\textquotedblleft}Postdoctoral Fellowship Implementation in Lithuania{\textquotedblright} . The study was funded from the European Community׳s Social Foundation under Grant Agreement no. VP1-3.1-{\v S}MM-08-K-01-004/KS-120000-1756 .",

year = "2014",

month = sep,

doi = "10.1016/j.ceramint.2014.04.120",

language = "English",

volume = "40",

pages = "12717--12722",

journal = "Ceramics International",

issn = "0272-8842",

publisher = "Elsevier Ltd",

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T1 - Calcium hydroxyapatite/whitlockite obtained from dairy products

T2 - Simple, environmentally benign and green preparation technology

AU - Trinkunaite-Felsen, J.

AU - Stankeviciute, Z.

AU - Yang, J. C.

AU - Yang, Thomas C.K.

AU - Beganskiene, A.

AU - Kareiva, A.

N1 - Funding Information: Postdoctoral fellowship of Z.S. is being funded by European Union Structural Funds Project “Postdoctoral Fellowship Implementation in Lithuania” . The study was funded from the European Community׳s Social Foundation under Grant Agreement no. VP1-3.1-ŠMM-08-K-01-004/KS-120000-1756 .

PY - 2014/9

Y1 - 2014/9

N2 - This study presents synthesis and characterization of calcium hydroxyapatite (Ca10(PO4)6(OH)2, CHAp) and whitlockite (Ca18Mg2H2(PO 4)14) composite obtained from dairy product. First, calcium containing powders were precipitated from whey permeate by combining the effect of alkaline pH and temperature. Subsequently a calcium containing phase was collected using membrane filtration and spray-dried. Finally, the temperature treatment was applied to eliminate the organic phase and purify calcium containing compounds. The mechanism of thermal decomposition of dairy calcium powder (DCP) was investigated using thermogravimetric analysis coupled with differential scanning calorimetry (TG-DSC). The phase composition, structural and morphological features of the final products were studied by X-ray diffraction analysis (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM).

AB - This study presents synthesis and characterization of calcium hydroxyapatite (Ca10(PO4)6(OH)2, CHAp) and whitlockite (Ca18Mg2H2(PO 4)14) composite obtained from dairy product. First, calcium containing powders were precipitated from whey permeate by combining the effect of alkaline pH and temperature. Subsequently a calcium containing phase was collected using membrane filtration and spray-dried. Finally, the temperature treatment was applied to eliminate the organic phase and purify calcium containing compounds. The mechanism of thermal decomposition of dairy calcium powder (DCP) was investigated using thermogravimetric analysis coupled with differential scanning calorimetry (TG-DSC). The phase composition, structural and morphological features of the final products were studied by X-ray diffraction analysis (XRD), Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM).

KW - Bioceramic materials

KW - Calcium hydroxyapatite

KW - Dairy products

KW - Green manufacturing

KW - Whitlockite

UR - https://www.scopus.com/pages/publications/84903878271

UR - https://www.scopus.com/pages/publications/84903878271#tab=citedBy

U2 - 10.1016/j.ceramint.2014.04.120

DO - 10.1016/j.ceramint.2014.04.120

M3 - Article

AN - SCOPUS:84903878271

SN - 0272-8842

VL - 40

SP - 12717

EP - 12722

JO - Ceramics International

JF - Ceramics International

IS - 8 PART B

ER -

Calcium hydroxyapatite/whitlockite obtained from dairy products: Simple, environmentally benign and green preparation technology

Abstract

UN SDGs

Keywords

ASJC Scopus subject areas

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